The sample is refrigerated by means of a cooling coil and collect 100 mL of liquid in a weathering tube, The sample allowed to evaporate ( “weather") at ambient pressure under specified conditions. When 5 mL of liquid test portion remains, the observed temperature is corrected for barometric pressure and thermometer ice point error, and reported as 95 % evaporation temperature.
The TCC-B D1837 is a bath for the determination of the relative purity of the various types of liquefied petroleum gases and is used to cool down the sample and to hold the weathering tube in a vertical position. The TCC-B D1837 is a single and adjustable circulator bath with position for one cooling coil. The accessories for tests in accordance with ASTM D1837 can also be supplied by Tamson.
The TCC-B is available in the following voltages/frequencies:
- TCC-B D1837 230V/50Hz (P/N: 00T0315)
- TCC-B D1837 230V/60Hz (P/N: 00T0316)
See tab "More Information" for the specificationsheet and manual
General:
Volatility, expressed in terms of the 95 % evaporated temperature of the product, is a measure of the amount of least volatile components present in the product. Coupled with a vapor pressure limit, it serves to ensure essentially single-component products in the cases of commercial grades of propane and butane. When the volatility is coupled with a vapor pressure limit which has been related to density, as in the case of the commercial PB-mixtures, the combination serves to assure essentially two component mixtures for such fuels. When coupled with a proper vapor pressure limit, this measurement serves to assure that special-duty propane products will be composed chiefly of propane and propylene, and that propane will be the major constituent. The presence of hydrocarbon compounds less volatile than those of which the LPG is primarily composed is indicated by an increase in the 95 % evaporated temperature. When the type and concentralion of higher boiling components is required, chromatographic analysis should be used.
Cooling coil—Approximately 6 m of 4.8 mm is wound in an outside diameter of 54 mm. The top of the coil is at least 25 mm below the top of the cooling vessel . The open ends of the coil shall are less than 100 mm. above as described per ASTM D1837. The downstream end of the coil is connected to a 3.2 mm. needle valve having an outlet connection not more than 76 mm long.
Test:
The sample is refrigerated by means of a cooling coil and collect 100 mL of liquid in a weathering tube, The sample allowed to evaporate ( “weather") at ambient pressure under specified conditions. When 5 mL of liquid test portion remains, the observed temperature is corrected for barometric pressure and thermometer ice point error, and reported as 95 % evaporation temperature.
Repeatability: 6°C(1.0°F)
Reproducibility: 1.0 (1.7°F) for butane and butane-propane mixtures
3°C(2.3°F)forpropane
This test method has no bias because the volatility is defined only in terms of this test method.
Differences between D1837 and D2158
|
Aspect |
D1837 |
D2158 |
|
Focus |
Evaporation Behavior |
Residue content |
|
Test type |
Functional |
Quantative |
|
Detects |
Poor volatility |
Nonvolatile contaminents |
|
Result |
Observation / behavior |
Mass of residue |
|
Purpose |
Performance |
Cleanliness |
Main Features:
- Holder to hold weathering tube in vertical position
- Wheels for easy transport
- Temperature range down to -85°C
- Level detection
- Stainless steel, robust bath
- Low energy consumption
- Easy to read display
- Very quiet
- High heat removal capacity
The TCC-B is available in the following voltages/frequencies:
- TCC-B D1837 230V/50Hz (P/N: 00T0315)
- TCC-B D1837 230V/60Hz (P/N: 00T0316)
See tab "More Information" for the specificationsheet and manual
| Bath_accuracy | 0.05°C |
|---|---|
| Bath Volume | 13 L |
| bath height | 900 mm |
| Bath Width | 380 mm |
| bath length | 770 mm |
| Bath Opening | 175 * 130 mm |
| bath depth | 240 mm |
| bath max temp | +20°C |
| Minimum Temperature | -85°C |
| Specification | click here |
| Manual | click here |
